S.I. No. 13/1978 - European Communities (Marketing of Fertilisers) Regulations, 1978.


S.I. No. 13 of 1978.

EUROPEAN COMMUNITIES (MARKETING OF FERTILISERS) REGULATIONS, 1978.

I, JAMES GIBBONS, Minister for Agriculture, in exercise of the powers conferred on me by section 3 of the European Communities Act, 1972 (No. 27 of 1972), for the purpose of giving effect to Council Directive No. 76/116/EEC hereby make the following regulations:

1 Short title and commencement.

1. These Regulations may be cited as the European Communities (Marketing of Fertilisers) Regulations, 1978 and shall come into effect on the 1st day of February, 1978.

2 Interpretation.

2. (1) In these Regulations:—

"Annex I" means Annex I to the directive;

"Annex II" means Annex II to the directive;

"authorised officer" means an officer of the Minister authorised in writing by the Minister for the purposes of these Regulations;

"the directive" means Council Directive No. 76/116/EEC of 18 December, 1975(a);

"Member State" means a Member State of the European Communities;

" the Minister" means the Minister for Agriculture;

"statute" has the same meaning as in section 3 of the Interpretation Act, 1937 (No. 38 of 1937);

"third country" means a country or territory which is not a Member State;

"State Chemist" means the head of the State Laboratory or a person authorised by him for the purposes of these Regulations.

(2) Any reference in these Regulations to place on the market or to marketing includes a reference to barter, offer or expose for sale by wholesale or retail, or have in possession for sale by wholesale or retail and invite to buy, and kindred words shall be construed accordingly.

(3) A word or expression that is used in these Regulations and is also used in the directive has, unless the contrary intention appears, the meaning in these Regulations that it has in the directive.

3 Application.

3. These Regulations apply to any fertiliser which is designated as "EEC fertiliser".

4 Marketing requirements and responsible person.

4. (1) A fertiliser to which these Regulations apply may not be marketed unless:—

(a) OJ No. L 24/21, 30 January, 1976.

( a ) it is a type of solid fertiliser specified in column (1) of Part I of the Schedule to these Regulations,

( b ) it is a product described in column (2) of the said Part I opposite the mention in the said column (1) of its type of solid fertiliser,

( c ) it complies with the requirements as to the minimum content of nutrients specified in column (3) of the said Part I opposite siuch mention and any other requirements so specified,

( d ) it complies with the requirements (if any) specified in column (4) and (5) of the said Part I opposite such mention,

( e ) there are given or used—

(i) the compulsory particulars mentioned in Part II of the said Schedule, and

(ii) the compulsory identification markings referred to in subparagraph (a), (b), (d) and (e) of paragraph 1 of Annex II to the directive,

( f ) in case the measured value of a nutrient contained in the fertiliser deviates from the nutrient's declared value, such deviation is within the relevant tolerances specified in Part III of the said Schedule,

( g ) in case the fertiliser is packaged, the provisions of Article 6 of the directive are complied with, and

( h ) the labelling requirements of paragraph (2) of the said Annex II are complied with in relation to it,

and such particulars and markings shall,

( i ) in case the quantity of fertiliser contained in a container does not exceed 100 kg., either be marked on the container or appear on a label attached to the container,

( j ) in case the quantity of fertiliser so contained exceeds 100 kg., or in case the fertiliser is supplied in bulk, appear on documents documents accompanying the fertiliser.

(2) A fertiliser to which these Regulations apply shall not be placed on the market if the markings on the packages or labels relating to it, or on the documents accompanying it and which so relate, are markings other than—

( a ) markings used for the purpose of complying with this Regulation,

( b ) optional data (if any) regarding the fertiliser which is data listed in column (4) or (5) of Part I of the Schedule to these Regulations opposite the mention of the relevant solid fertiliser type,

( c ) a mark or description mentioned in Article 4 (1) (c) of the directive,

( d ) a direction mentioned in Article 4 (1) (d) of the directive, or

( e ) markings permitted or required to be used by any act of the European Communities or by any statutory instrument made under section 3 of the European Communities Act, 1972 (No. 27 of 1972), other than these Regulations.

(3) In addition to the foregoing, the following requirements shall be complied with, namely—

( a ) the indications referred to in subparagraphs (c) and (d) of paragraph (2) of this Regulation, or either of them, shall, if if used, not conflict with, and shall be clearly separated from, the markings mentioned in subparagraph (a) of the said paragraph (2) and, where used, the data mentioned in subparagraph (b) of that paragraph, and

( b ) the markings and particulars referred to in paragraph (1) (e) of of this Regulation, any data which is data referred to in the said subparagraph (b), any mark or description which is a mark or description referred to in the said subparagraph (c) and any direction which is a direction referred to in the said subparagraph (d) shall be clearly separated from any other information on packages containing, or labels or other documents used in relation to a fertiliser to which these Regulations apply.

(4) The indications, markings or data mentioned in paragraph (2) of this Regulation shall, when given or used, be at least in the Irish language or the English language.

(5) A person who contravenes any of the foregoing provisions of this Regulation shall be guilty of an offence and shall be liable on summary conviction to a fine not exceeding £200 or, at the discretion of the Court, to imprisonment for a term not exceeding six months.

5 Sampling on request.

5. (1) Where a person has on his premises any fertiliser to which these Regulations apply which he has purchased and which he proposes to use in the course of his farming operations, he may apply in writing to the Minister to have a sample thereof taken for analysis.

(2) An application under this Regulation shall be—

( a ) made in writing within the period of twenty-eight days beginning on the date on which the fertiliser to which the application relates was delivered to the applicant, and

( b ) accompanied by a fee of £5.

(3) Where an application is duly made under this Regulation, an (authorised officer shall, subject to paragraph (4) of this Regulation, take in accordance with Regulation 3 of the European Communities Sampling and Analysis of Fertilisers) Regulations, 1978, and thereafter transmit to the State Chemist, a sample of the fertiliser to which the application relates.

(4) Where an application is made under this Regulation, the following provisions shall apply:

( a ) an authorised officer shall not take a sample after the expiration of the period of forty-two days beginning on the date on which the relevant fertiliser was delivered to the applicant,

( b ) an authorised officer may, if he thinks fit, decline to take a sample if—

(i) he is not satisfied that the applicant has purchased such fertiliser, or

(ii) he is not satisfied that the applicant proposes to use such fertiliser in the course of his farming operations, or

(iii) he is not satisfied that such fertiliser as presented for sampling is fairly representative of the fertiliser as delivered to the applicant, or

(iv) the applicant does not furnish such information relating to such fertiliser as the authorised officer may require.

(5) Where the State Chemist receives a sample taken in pursuance of an application under this Regulation, he shall comply with the requirements of Regulation 4 of the European Communities (Sampling and Analysis of Fertilisers) Regulations, 1978, and shall send to the applicant a certificate, in the form set out in Part IV of the Schedule to these Regulations, of the result of the analysis.

(6) Subject to paragraph (7) of this Regulation, all fees under this Regulation shall be paid into or disposed of for the benefit of the Exchequer in accordance with the directions of the Minister for Finance and, accordingly, the Public Offices Fees Act, 1879, shall not apply in respect thereof.

(7) In any case in which he considers it proper so to do (not being a case in which the applicant has received a certificate under this Regulation), the Minister may refund a fee paid in relation to an application under this Regulation.

(8) For the purpose of this Regulation a fertiliser shall not be regarded as having been delivered to a purchaser unless it arrives at the destination to which it is consigned, whether the consignment is by direction of the supplier or the purchaser.

6 Records returns etc.

6. (1) Every person who carries on, or is employed in connection with, the business of manufacturing, importing or marketing fertiliser which is designated "EEC fertiliser" shall—

( a ) keep records of his transactions in such fertiliser;

( b ) produce at the request of an authorised officer any books, documents or records relating to such business which are in the possession or under the control of such person;

( c ) permit an authorised officer to inspect and take extracts from such books, documents or records and give to the officer any information which he may reasonably require in relation to any entries therein;

( d ) afford to an authorised officer reasonable facilities for inspecting the stock of any such fertiliser which is for the time being on any premises on which such person carries on such a business;

( e ) give to an authorised officer any information he may reasonably require in relation to such transactions including in particular information which he may reasonably require regarding any fertiliser which is so designated and is specified by him.

(2) A person who contravenes any of the provisions of paragraph (1) of this Regulation shall be guilty of an offence and shall be liable on summary conviction to a fine not exceeding £200 or, at the discretion of the Court, to imprisonment for a term not exceeding six months.

7 Powers of authorised officers.

7. (1) In addition to the powers conferred by Regulation 6 of these Regulations an authorised officer may at all reasonable times enter and inspect any premises, railway wagon, vehicle, ship, vessel, aircraft or other thing (e.g. a container) used to transport in which he has reasonable grounds for believing that any fertiliser to which these Regulations apply is being marketed, manufactured for sale, imported, stored or kept for sale or sold and may examine and take samples of any fertiliser designated as "EEC fertiliser" which he finds in the course of his inspection.

(2) In any proceedings for an offence under these Regulations evidence of the result of analysis of a sample taken under these Regulations may be given if it is proved that—

( a ) the sample was taken in accordance with the European Communities (Sampling and Analysis of Fertilisers) Regulations, 1978,

( b ) the analysis was carried out in accordance with the said Regulations,

and, save as aforesaid, evidence of the result of such an analysis shall not be given in any such proceedings.

(3) Any person who obstructs or interferes with an authorised officer in the course of exercising a power conferred on him under this Regulation shall be guilty of an offence and shall be liable on summary conviction to a fine not exceeding £100.

(4) The Minister shall furnish an authorised officer with a certificate of his appointment and, when exercising any powers conferred by these Regulations, the officer shall if requested by any person affected, produce the certificate to that person.

8 Power to publish results of analyses.

8. The Minister may at his decretion publish the result of any analysis to made by reason either of an application under Regulation 5 or of the taking of a sample pursuant to Regulation 7 of these Regulations.

9 Certificate of analysis as evidence.

9. In any legal proceedings the production of a certificate in the form specified in Part IV of the Schedule to these Regulations and purporting to be signed by the State Chemist shall be sufficient evidence of the facts stated in the certificate and of the analysis having been carried out in accordance with the European Communities (Sampling and Analysis of Fertilisers) Regulations, 1978, unless either party requires the person who made the analysis to be called as a witness.

10 Tampering with sample s.

10. If any person fraudulently—

( a ) tampers with any thing so as to procure that any sample taken pursuant to Regulations 5 or 7 of these Regulations does not correctly represent the substance sampled, or

( b ) tampers or interferes with any sample taken under these Regulations,

he shall be guilty of an offence and shall be liable on summary conviction to a fine not exceeding £100 or, at the discretion of the court, to imprisonment for a term not exceeding six months.

11 Additional responsible person.

11. (1) ( a ) Where a fertiliser is placed on the market in contravention of Regulation 4 of these Regulations by a person other than the person who in relation to the fertiliser is the person described in paragraph 1 (e) of Annex II to the directive, then the person so described shall, if at the time of the contravention he has a place of business in the State, also be guilty of an offence.

( b ) Where—

(i) a fertiliser is placed on the market in contravention of Regulation 4 of these Regulations by a person other than the person who in relation to the fertiliser is the person so described, and

(ii) the fertiliser is imported fertiliser and is so placed on the market by a person other than the importer,

then the person by whom the fertiliser was imported shall also be guilty of an offence.

(2) Proceedings for an offence under this Regulation, and for an offence under Regulation 4 of these Regulations shall not be brought in respect of the same act.

(3) ( a ) In any proceedings for an offence under this Regulation it shall be a defence for a defendant to prove that he took reasonable steps to avoid the relevant fertiliser being placed on the market in contravention of Regulation 4 of these Regulations.

( b ) In any proceedings for an offence under paragraph (1) (b) of this Regulation it shall be a defence for the defendant to prove that at the time of the contravention the person who in relation to the fertiliser concerned is the person described in paragraph (1) (e) of Annex II to the directive had a place of business in the State.

(4) A person guilty of an offence under this Regulation shall be liable on summary conviction to a fine not exceeding £200 or, at the discretion of the Court, to imprisonment for a term not exceeding six months.

12 Prosecution of offences.

12. An offence under these Regulations may be prosecuted by the Minister.

13 Saver.

13. Nothing in these Regulations shall be construed as affecting a provision of any statute, whether passed before or after the making of these Regulations, which is a provision for the protection of human life or health, animal life or health, plant life or health or industrial or commercial property.

14 Amendment of Fertilisers, Feedingstuffs and Mineral Mixtures Regulations, 1957.

14. The Fertilisers, Feedingstuffs and Mineral Mixtures Regulations, 1957 ( S.I. No. 264 of 1957 ), shall not apply to any fertiliser to which these Regulations apply.

SCHEDULE.

PART 1.

Data required or permitted to be used by these Regulations.

A. STRAIGHT FERTILISERS.

1. NITROGENOUS FERTILISERS.

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Calcium nitrate (nitrate of lime)

Chemically obtained product containing calcium nitrate as its essential ingredient and possibly ammonium nitrate

15% N

Nitrogen expressed as total nitrogen or as nitric and ammoniacal nitrogen.

Maximum content of ammoniacal nitrogen: 1·5% N

Total nitrogen

Additional optional particulars: Nitric nitrogen Ammoniacal nitrogen

Calcium magnesium nitrate (nitrate of lime and magnesium)

Chemically obtained product containing calcium nitrate and magnesium nitrate as essential ingredients

13% N

Nitrogen expressed as nitric nitrogen. Minimum content magnesium in the form of water-soluble salts expressed as magnesium: 3% Mg

Nitric nitrogen

Water-soluble magesium salts expressed as magnesium

Sodium nitrate (nitrate of soda)

Chemically obtained product containing sodium nitrate as its essential ingredient

15% N

Nitrogen expressed as nitric nitrogen

Nitric nitrogen

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Chile nitrate

Product prepared from caliche, containing sodium nitrate as its essential ingredient

15% N

Nitrogen expressed as nitric nitrogen

Nitric nitrogen

Calcium Cyanamide

Chemically obtained product containing calcium cyanamide as its essential ingredient, calcium oxide and possibly small quantities of ammonium salts and urea

18% N

Nitrogen expressed as total nitrogen, at least 75% of the nitrogen declared being bound in the form of cyanamide

Total nitrogen

Nitrogenous calcium cyanamide

Chemically obtained product containing calcium cyanamide as its essential ingredient, and calcium oxide and possibly small quantities of ammonium salts and urea, plus added nitrate

18% N

Nitrogen expressed as total nitrogen, at least 75% of the non-nitric nitrogen declared being bound in the form of cyanamide. Nitric nitrogen content:

minimum: 1% N

maximum: 3% N

Total nitrogen

Nitric nitrogen

Sulphate of ammonia

Chemically obtained product containing ammonium sulphate as its essential ingredient

20% N

Nitrogen expressed as ammoniacal nitrogen

Ammoniacal nitrogen

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Ammonium nitrate or calcium ammonium nitrate

Chemically obtained product nitrate as its essential ingredient, which may contain fillers such as ground limestone, calcium sulphate, ground dolomite, magnesium sulphate, kieserite

20% N

Nitrogen expressed as nitric nitrogen and ammoniacal nitrogen, each of these two forms of nitrogen accounting for about half the nitrogen present

The designation 'calcium ammonium nitrate' is exclusively reserved for a fertiliser containing only calcium carbonate (limestone) and/or magnesium carbonate and calcium carbonate (dolomite) in addition to ammonium nitrate. The minimum content of these carbonates must be 20% and their purity level at least 90%

Total nitrogen

Nitric nitrogen

Ammoniacal nitrogen

Ammonium sulphate-nitrate

Chemically obtained product containing as essential ingredients ammonium nitrate and ammonium sulphate

25% N

Nitrogen expressed as ammoniacal and nitric nitrogen. Minimum nitric nitrogen content: 5%

Total nitrogen

Ammoniacal nitrogen

Nitric nitrogen

Magnesium sulphonitrate

Chemically obtained product containing ammonium nitrate, ammonium sulphate and magnesium sulphate as essential ingredients

19% N

Nitrogen expressed as ammoniacal and nitric nitrogen. Minimum nitric nitrogen content;

6% N; 3% Mg

Watersoluble magnesium salts expressed as magnesium

Total nitrogen

Ammoniacal nitrogen

Nitric nitrogen

Water-soluble

magnesium salts expressed as magnesium

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Magnesium ammonium nitrate

Chemically obtained product containing ammonium nitrates and magnesium compound salts (dolomite magnesium carbonate and/or magnesium sulphate) as essential ingredients

19% N

Nitrogen expressed as ammoniacal nitrogen and nitric nitrogen. Minimum nitric nitrogen content: 6% N 3% Mg

Magnesium expressed as total magnesium

Total nitrogen

Ammoniacal nitrogen

Nitric nitrogen

Total magnesium

Urea

Chemically obtained product containing carbonyl diamide (carbamide) as its essential ingredient

44% N

Total ureic nitrogen (including biuret). Maximum biuret content: 1·2%

Total nitrogen,

expressed as ureic nitrogen

II PHOSPHATIC FERTILISERS

Where a particle size criterion is prescribed for the basic constituent materials of fertilisers sold in granular form it will be established by an appropriate analytical method.

Basic Slag

—Thomas phosphates

—Thomas slag

Product obtained in iron-smelting by treatment of the phosphorus melts and containing calcium silicophosphates as its essential ingredients

5·2% P

Phosphorus soluble in mineral acids, at least 75% of the declared content of phosphorus being soluble in 2% citric acid; or

Phosphorus soluble in 2% citric acid

4·4% P

Phosphorus soluble in 2% citric acid

Particle size:

at least 75% able to pass through a sieve with a mesh of 0·160 mm, at least 96% able to pass through a sieve with a mesh of 0·630 mm

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Normal superphosphate

Product obtained by reaction of ground mineral phosphate with sulphuric acid and containing monocalcium phosphate as an essential ingredient as well as calcium sulphate

7% P

Phosphorus soluble in neutral ammonium citrate, at least 93% of the declared content of P being water-soluble

Test sample: 1 g

Phosphorus soluble in neutral ammonium citrate

Water-soluble phosphorus

Concentrated superphosphate

Product obtained by reaction of ground mineral phosphate with sulphuric acid and phosphoric acid and containing monocalcium phosphate as an essential ingredient as well as calcium sulphate

11% P

Phosphorus soluble in neutral ammonium citrate, at least 93% of the declared content of P being water-soluble

Test sample: 1 g

Phosphorus soluble in neutral ammonium citrate

Water-soluble phosphorus

Triple superphosphate

Product obtained by reaction of ground mineral phosphate with phosphoric acid and containing monocalcium phosphate as its essential ingredient

16·5% P

Phosporus soluble in neutral ammonium citrate, at least 93 % of the declared content of P being water-soluble

Test sample: 3 g

Phosphorus soluble in neutral ammonium citrate

Water-soluble phosphorus

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Partially solubilized rock phosphate

Product obtained by partial solubilization of ground rock phosphate with sulphuric acid or phosphoric acid and containing as essential ingredients monocalcium phosphate, tricalcium phosphate and calcium sulphate

8·5% P

Phosphorus soluble in mineral acids, at least 40% of the declared content of P being water-soluble

Particle size:

—at least 90% able to pass through a sieve with a mesh of 0·160 m

—at least 98% able to pass through a sieve with a mesh of 0·630 mm

Total phosphorus (soluble in mineral acids)

Phosphorus soluble in water

Dicalcium phosphate

Product obtained by precipitation of solubilized phosphoric acid from mineral phosphates or bones, and containing dicalcium phosphate dihydrate as its essential ingredient

16·5% P

Phosphorus soluble in alkaline ammonium citrate (Petermann)

Particle size:

—at least 90% able to pass through a sieve with a mesh of 0·160 mm

—at least 98% able to pass through a sieve with a mesh of 0·630 mm

Phosphorus soluble in alkaline ammonium citrate

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Calcined phosphate

Product obtained by heat treatment of ground rock phosphate with alkaline compounds and silicic acid, and containing alkaline calcium phosphate and calcium silicate as essential ingredients

11% P

Phosphorus soluble in alkaline ammonium citrate (Petermann)

Particle size

—at least 75% able to pass through a sieve with a mesh of 0·160 mm

—at least 96% able to pass through a sieve with a mesh of 0·630 mm

Phosphorus soluble in alkaline ammonium citrate

Aluminium-calcium phosphate

Product obtained in amorphous form by heat treatment and grinding, containing aluminium and calcium phosphates as essential ingredients

13% P

Phosphorus soluble in mineral acids, at least 75 % of the declared content of P being soluble in alkaline ammonium citrate (Joulie)

Particle size:

—at least 90% able to pass through a sieve with a mesh of 0·160 mm

—at least 98% able to pass through a sieve with a mesh of 0·630 mm

Total phosphorus (soluble in mineral acids)

Phosphorus soluble in alkaline ammonium citrate

Type designation

Data on method of production and essential ingredients

Minimum content of nutrients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Soft ground rock phosphate

Product obtained by grinding soft mineral phosphates and containing tricalcium phosphate and calcium carbonate as essential ingredients

11% P

Phosphorus soluble in mineral acids, at least 55 % of the declared content of P being soluble in 2% formic acid

Particle size:

— at least 90% able to pass through a sieve with a mesh of 0·063 mm

—at least 99% able to pass through a sieve with a mesh of 0·125 mm

Total phosphorus (soluble in mineral acids)

Phosphorus soluble in 2% formic acid

Percentage by weight of material able to pass through a sieve with a mesh of 0·063 mm

III. POTASSIC FERTILISERS

Kainit

Product obtained from crude potassium salts

8·5% K

Water-soluble potassium 3% Mg

Magnesium in the form of water-soluble salts, expressed as magnesium

Usual trade names may be added

Water-soluble potassium

Water-soluble magnesium salts expressed as magnesium

Enriched kainit salt

Product obtained from crude potassium salts enriched by blending with potassium chloride.

15% K

Water-soluble potassium

Usual trade names may be added

Water-soluble potassium

Optional mention of the water-soluble magnesium content when higher than 3% Mg

Type designation

Data on method of production and essential ingredients

Minimum content of nuttients (percentage by weight); data on the expression of nutrients; other requirements

Other data on the type designation

Nutrient content to be declared; forms and solubilities of the nutrients; other criteria

(1)

(2)

(3)

(4)

(5)

Muriate of potash

Product obtained from crude potassium salts and containing potassium chloride as its essential ingredient

30·5% K

Water-soluble potassium

Usual trade names may be added

Water-soluble potassium

Potassium chloride containing magnesium salt

Product obtained from crude potassium salts with added magnesium salts and containing potassium chloride and magnesium salts as essential ingredients

30·5% K

Water-soluble potassium

3% Mg

Magnesium in the form of water-soluble salts, expressed as magnesium

Water-soluble potassium

Water-soluble magnesium salts expressed as magnesium

Sulphate of potash

Product obtained chemically from potassium salts and containing potassium sulphate as its essential ingredient

39% K

Water-soluble potassium

Maximum chlorine content:

3% Cl

Water-soluble potassium

Optional mention of the chlorine content where lower than 3 % Cl

Sulphate of potash containing magnesium salt

Product obtained chemically from potassium salts possibly with addition of magnesium salts, and containing potassium sulphate and magnesium sulphate as essential ingredients

18·5% K

Water-soluble potassium

4·8% Mg

Magnesium in the form of water-soluble salts, expressed as magnesium

Maximum chlorine content: 3% Cl

Usual trade names may be added

Water-soluble potassium Water-soluble magnesium salts expressed as magnesium

Optional mention of the chlorine content where lower than 3% Cl

B. COMPOUND FERTILISER TYPES.

1. NPK FERTILISERS.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements.

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

NPK Fertiliser

Product obtained chemically or by blending, without addition of organic nutrients of animal or vegetable origin

20%* (N + P + K)

3% N

2·18% P

4·15% K

(1) Total nitrogen

(2) Nitric nitrogen

(3) Ammonical nitrogen

(4) Ureic nitrogen

(5) Cyanamide nitrogen

(1) Water-soluble P

(2) P soluble in neutral ammonium citrate

(3) P soluble in neutral ammonium citrate and in water

(4) P soluble in mineral acids only

(5) P soluble in alkaline ammonium citrate (Petermann)

(6a) P soluble in mineral acids, of which at least 75% of the declared P content is soluble in 2% citric acid

(6b) P soluble in 2% citric acid (7) P soluble in mineral acids, of which at least 75% of the declared P content is soluble in alkaline ammonium citrate (Joulie)

Water- solubleK

(1) Total nitrogen

(2) If any of the forms of nitrogen (2) to (5)amounts to at least 1% by weight, it must be declared

1. An NPK fertiliser free from Thomas slag, calcined phosphate, partially solubilized rock phosphate and soft ground rock phosphate must be declared in accordance with solubilities (1), (2) or (3):

(1) Water-soluble

potassium

(2) The indication 'low in chlorine' is linked to a maximum content of 2% Cl.

(3) Chlorine content may be declared.

— when the water-soluble P does not amount to ·87% solubility (2) only shall be declared;

—when the water-soluble P is at least ·87% solubility (3) shall be declared, and the water-soluble P content must be indicated (solubility (1)). The P content soluble in mineral acids only must not exceed ·87%.

*20% (N+P+K) to be calculated by multiplying the nutrient contents N, P, and K by 1, 2·29 and 1·2 respectively and adding the results of such multiplication.

Type designation

Data on method of production

Minimum of content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

which at least 75% of the declared P content is soluble in alkaline ammonium citrate (Joulie)

For this type 1, the test sample for determining solubilities (2) and (3) shall be 1g.

2. (a) An NPK fertiliser containing soft ground rock phosphate or partially solubilized rock phosphate must be free from Thomas slag, calcined phosphate and aluminium-calcium phosphate. It shall be declared in accordance with solubilities (1), (3) and (4).

This type of fertiliser must contain:

—at least ·87% P soluble in mineral acids only (solubility (4));

—at least 2·2% P soluble in water and neutral ammonium citrate (solubility (3));

—at least 1·1% water-soluble P (solubility (1)).

This type of fertiliser must be marketed under the designation 'NPK fertiliser containing soft ground rock phosphate' or 'NPK fertiliser containing partially solubilised rock phosphate'. For this type 2(a), the test sample for determining solubility (3) shall be 3 g.

(8) P soluble in minerals acids, of which at least 55% of the declared P content is soluble in 2% formic acid

Particle size of the basic phosphatic ingredients:

Thomas slag: at least 75% able to pass through a sieve with a mesh of 0·63 mm.

Aluminium-calcium phosphate:at least 90% able to pass through a sieve with a mesh of 0·160mm.

Calcined phosphate: at least 75% able to pass through a sieve with a mesh of 0·160 mm.

Soft ground rock phosphate: at least 90% able to pass through a sieve with a mesh of 0·063 mm.

Partially solubilized rock phosphate: at least 90% able to pass through a sieve with a mesh of 0·160mm

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

2. (b) An NPK fertiliser containing aluminium-calcium phosphate must be free from Thomas Slag, calcined phosphate, soft ground rock phosphate and partially solubilized rock phosphate.

It shall be declared in accordance with solubilities (1) and (7), the latter applying after deduction of the solubility in water. This type of fertiliser must contain:

—at least ·87 % of water-soluble P (solubility (1)):

—at least 22% of P according to solubility (7). This type of fertiliser must be marketed under the designation 'NPK fertiliser containing aluminium-calcium phosphate.

3. In the case of the NPK fertilisers containing only one of the following types of phosphatic fertiliser:

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements.

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

Thomas slag, calcined phosphate aluminium-calcium phosphate, soft ground rock phosphate, the type designation must be followed by an indication of the phosphate ingredient.

The declaration of the solubility of the P must be given in accordance with the following solubilities:

—for fertilisers based on Thomas slag:

solubility (6b);

—for fertilisers based on calcined phosphate:

solubility (5);

—for fertilisers based on aluminium-calcium phosphate:

solubility (7);

—for fertilisers based on soft ground rock phosphate:

solubility (8).

2. NP FERTILISERS.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

NP Fertiliser

Product obtained chemically or by blending without addition of organic nutrients of animal or vegetable origin.

18% (N+P)*

3% N 2·18% P

(1) Total Nitrogen

(2) Nitric nitrogen

(3) Ammoniacal nitrogen

(4) Ureic nitrogen

(5) Cyanamide nitrogen

(1) Water-soluble P

(2) P soluble in neutral ammonium citrate

(3) P soluble in neutral ammonium citrate and in water.

(4) P soluble in mineral acids only

(5) P soluble in alkaline ammonium citrate (Petermann)

(6a) P soluble in mineral acids of which at least 75% of the declared P content is soluble in 2% citric acid

(1) Total nitrogen

(2) If any of the forms of nitrogen (2) to (5) amounts to at least 1% by weight it must be declared

1. An NP fertiliser free from Thomas slag, calcined phosphate, aluminium calcium phosphate, partially solubilized rock phosphate and soft ground rock phosphate must be declared in accordance with solubilities (1), (2) or (3):

—when the water-soluble P does not amount to ·87% solubility (2) only shall be declared:

—when the water-soluble P is at least ·87%, solubility (3) shall be declared, and the water-soluble P content must be indicated (solubility (1)).

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements.

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

(6b) P soluble in 2% citric acid

The P content soluble in mineral acids only must not exceed ·87%.

For this type 1, the test sample for determining solubilities (2) and (3) shall be 1 g.

For this type 1, the test sample for determining solubilities (2) and (3) shall be 1 g.

2(a). An NP fertiliser containing soft ground rock phosphate or partially solubilized rock phosphate must be free from Thomas slag, calcined phosphate and aluminium-calcium phosphate.

It shall be declared in accordance with solubilities (1), (3) and (4).

(7) P soluble in mineral acids of which at least 75% of the declared P content is soluble in alkaline ammonium citrate (Joulie)

(8) P soluble in mineral acids of which at least 55% of the declared P content is soluble in 2 % formic acid 55% of the declared P content is soluble in 2% formic acid

This type of fertiliser must contain:

—at least 87 %P soluble in mineral acids only (solubility (4));

—at least 2·2% P soluble in water and neutral ammonium citrate (solubility (3));

—at least 1·1% water-soluble P (solubility (1)).

This type of fertiliser must br marketed under the designation 'NP fertiliser containing soft ground rock phosphate' or 'NP fertiliser containing partially solubilized rock phosphate!

For this type 2 (a), the test sample for determining solubility (3) shall be 3 g.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements

(1)

(2)

(3)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

55% of the declared P content is soluble in 2% formic acid

rock phosphate' or `NP fertiliser containing partially solubilized rock phosphate!

For this type 2(a), the test sample for determining solubility (3) shall be 3 g.

Particle size of the basic phosphatic ingredients:

Thomas slag:

Aluminium-calcium phosphate:

Calcined phosphate:

Soft ground rock phosphate:

Partially solubilized rock phosphate:

at least 75% able to pass through a sieve with a mesh of 0·160 mm.

at least 90% able to pass through a sieve with a mesh of 0·160 mm.

at least 75% able to pass through a sieve with mesh of 0·160 mm.

at least 90% able to pass through a sieve with a mesh of 0·063 mm.

at least 90% able to pass through a sieve with a mesh of 0·160 mm.

2(b) An NP fertiliser containing alumium-calcium phosphate must be free from Thomas slag, calcined phosphate soft ground rock phosphate and partially solubilized rock phosphate.

It shall be declared in accordance with solubilities (1) and (7), the latter applying after deduction of the solubility in water.

This type of fertiliser must contain:

—at least ·87% water-soluble P (solubility (1));

—at least 2·2% P according to solubility (7).

This type of fertiliser must be marketed under the designation 'NP fertiliser containing aluminium-calcium phosphate'.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

3. In the case of NP fertilisers containing only one of the following types of phosphatic fertiliser:

Thomas slag, calcined phosphate, aluminium-calcium phosphate, soft ground rock phosphate, the type designation must be followed by an indication of the phosphate ingredient.

The declaration of the solubility of the P must be given in accordance with the following solubilities:

—for fertilisers based on Thomas slag: solubility (6b);

—for fertilisers based on calcined phosphate: solubility (5);

—for fertilisers based on aluminium-calcium phosphate: solubility (7);

—for fertilisers based on soft ground rock phosphate: solubility (8).

*18% (N+P) to be calculated by multiplying the nutrient contents N and P by 1 and 2·29 respectively and adding the results of such multiplication.

3. NK FERTILISERS.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertiliser; other requirements

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

NK Fertiliser

Product obtained chemically or by blending, without addition of organic nutrients of animal or vegetable origin

18% * (N+K.)

3% N

4·15% K

(1) Total nitrogen

(2) Nitric nitrogen

(3) Ammoniacal nitrogen

(4) Ureic nitrogen

(5) Cyanamide nitrogen

Water-soluble K

(1) Total nitrogen

(2) If any of the forms of nitrogen (2) to (5) amounts to at least 1 % by weight it must be declared

(1) Water-soluble potassium

(2) The indication 'low in chlorine' is linked to a maximum content of 2%/Cl.

(3) Chlorine content may be declared

*18 % (N+K) to be calculated by multiplying the nutrient contents N and K by 1 and 1·2 respectively and adding the results of such multiplication.

4. PK FERTILISERS.

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

PK Fertiliser

Product obtained chemically or by blending, without addition of organic nutrients of animal or vegetable origin

18%* (P+K)

2·18% P 4·15% K

(1) Water-soluble P

(2) P soluble in neutral ammonium citrate

(3) P soluble in neutral ammonium citrate and in water

(4) P soluble in mineral acids only

(5) P soluble in alkaline ammonium citrate (Petermann)

(6a) P soluble in mineral acids of which at least 75% of the declared P content is soluble in 2% citric acid.

(6b) P soluble in 2% citric acid

(7) P soluble in mineral acids of which at least 75% of the declared P content is soluble in alkaline ammonium citrate (Joulie)

(8) P soluble in mineral acids, of which at least 55% of the declared P content is soluble in 2% formic acid declared P content is soluble in 2% formic acid

Water-soluble K

1. A PK fertiliser free from Thomas slag, calcined phosphate, aluminium-calcium phosphate, partially solubilized rock phosphate and soft ground rock phosphate must be declared in accordance with solubilities (1), (2) or (3):

—when the water-soluble P does not amount to 87 % solubility (2) only shall be declared;

—when the water-soluble P is at least ·87% solubility (3) shall be declared and the water-soluble P content must be indicated (solubility (1)).

The P content soluble in mineral only must not exceed ·87 %

For this type 1, the test sample for determining solubilities (2) and (3) shall be 1 g.

2(a). A PK fertiliser containing soft ground rock phosphate or partially solubilized rock phosphate must be free from Thomas slag, calcined phosphate and aluminium-calcium phosphate,

It shall be declared in accordance with solubilities (1) (3) and (4). This type of fertiliser must contain:

—at least ·87% P soluble in mineral acids only (solubility (4));

—at least 2·2% P soluble in water and neutral ammonium citrate (solubility (3));

—at least 1·1% water-soluble P (solubility (1)).

This type of fertiliser must be marketed under the designation 'PK fertiliser containing soft ground rock phosphate' or 'PK fertiliser containing partially solubilized rock phosphate'.

Type designation

Data on method of production

Minimum content of nutrients (percentage by weight)

Forms, solubilities and nutrient content to be declared as specified in column 5; particle size.

Data for identification of the fertilisers; other requirements.

(1)

(2)

(3)

(4)

(5)

Total

For each of the nutrients

N

P

K

N

P

K

Particle size of the basic phosphatic ingredients:

For this type 2(a), the test sasmple for determining solubility (3) shall be 3 g

2(b). A PK. fertiliser containing aluminium-calcium phosphate must be free from Thomas slag, calcined phosphate and partially solubilized rock phosphate.

It shall be declared in accordance with solubilities (1) and (7), the latter applying after deduction of the solubility in water.

This type of fertiliser must contain:

—at least 87% water soluble P (solubility (1));

—at least 22% P according to solubility (7).

This type of fertiliser must be marketed under the designation 'PK fertiliser containing aluminium calcium phosphate'.

3. In the case of PK fertilisers containing only one of the following types of phosphatic fertiliser:

Thomas slag, calcined phosphate, aluminium-calcium phosphate, soft ground rock phosphate, the type designation must be followed by an indication of the phosphate ingredient.

The declaration of the solubility of the P must be given in accordance with the following solubilities:

—for fertilisers based on Thomas slag; solubility (6b);

—for fertilisers based on calcined phosphate: solubility (5);

—for fertilisers based on aluminium calcium phosphate: solubility (7);

—for fertilisers based on soft ground rock phosphate: solubility (8).

Thomas slag:

at least 75% able to pass through a sieve with a mesh of' 0·160 mm

Aluminium-calcium phosphate:

at least 90% able to pass through a sieve with a mesh of 0·160 mm

Calcined phosphate:

at least 75% able to pass through a sieve with a mesh of 0·160 mm

Soft ground rock phosphate:

at least 90% able to pass through a sieve with a mesh at least of 0.063 mm

Partially solubilized rock phosphate:

at least 90% able to pass through a sieve with a mesh of 0·160 mm

*18% (P+K) to be calculated by multiplying the nutrient contents P and K by 2·29 and 1·2 respectively and adding the results of such multiplication.

PART II.

PARTICULARS REFERRED TO IN REGULATION 4 (1) (e) (i).

( a ) The declared content in respect of each nutrient must be given; and the declared content expressed as forms and/or solubilities where those are specified in Annex I must also be given.

( b ) The nutrient content for straight and compound fertilisers must be given as a percentage by weight, as whole numbers or, where necessary, to one decimal place and for compound fertilisers in the following order, N, P and K.

( c ) The forms and solubilities of the nutrients must also be expressed as a percentage by weight of fertiliser, except where Annex I explicitly provides that this content shall be otherwise expressed.

( d ) Nutrients must be indicated both in words and by the appropriate chemical symbols (e.g. nitrogen (N), phosphorus (P), potassium (K), magnesium (Mg)).

PART III

TOLERANCES

( a ) The tolerances given in this Part are the permitted deviation of the measured value of a nutrient from its declared value.

( b ) They are intended to accommodate variations in manufacturing, sampling and analysis.

( c ) No tolerances are allowed in respect of the minimum and maximum contents specified in Annex I.

( d ) Where no maximum is given there are no restrictions on an excess of nutrient above the declared amount.

( e ) The tolerance allowed in respect of the declared nutrient contents in the various types of fertiliser are as follows:

A. STRAIGHT FERTILISERS:

absolute value in percentage by weight expressed as N, P, K, Mg, Cl

I. Nitrogenous fertilisers

calcium nitrate

0·4

calcium-magnesium nitrate

0·4

sodium nitrate

0·4

chile nitrate

0·4

calcium cyanamide

1·0

nitrogenous calcium cyanamide

1·0

ammonium sulphate

0·3

Ammonium nitrate or calcium ammonium: nitrate

—up to and including 32 %

0·8

—more than 32%

0·6

ammonium sulphate-nitrate

0·8

magnesium sulphonitrate

0·8

magnesium ammonium nitrate

0·8

urea

0·4

II. Phosphatic fertilisers

Thomas slag:

—declaration expressed as a range of 2% by weight

0

declaration expressed as a single number

0·44

Other phosphatic fertilisers

P solubility in: (number of fertiliser in Annex 1)

—mineral acid

(3, 6, 7)

0·35

—formic acid

(7)

0·35

—neutral ammonium citrate

(2a, 2b, 2c)

0·35

—alkaline ammonium citrate

(4, 5, 6)

0·35

—water

(2a, 2b, 3)

0·40

(2c)

0·57

III. Potassic fertilisers

kainit

1·25

enriched kainit salt

0·83

muriate of potash:

—up to and including 45%

0·83

—more than 45%

0·415

potassium chloride containing magnesium salt

1·25

sulphate of potash

0·415

sulphate of potash containing magnesium salt

1·25

Other components

magnesium

0·54

chlorine

0·2

B. COMPOUND FERTILISERS:

absolute value in percentage by weight expressed as N, P, K, Mg, Cl

1. Nutrient elements

—N

1·1

—P

0·48

—K

0·91

2. Total negative deviations from the declared value

—binary fertilisers

NP,

N+2·29P

1·5

NK,

N+1·2K

1·5

PK,

2·29P+1·2K

1·5

—ternary fertilisers

N+2·29P+1·2K

1·9

( f ) The tolerance allowed in respect of the declared content for the various forms of nitrogen is one-tenth of the overall content of the nutrient concerned with a maximum of 2 % by weight, provided that the overall content of that nutrient remains within the limits specified in Annex I and the tolerances specified in paragraph (e) above.

The tolerance allowed in respect of the declared solubilities of phosphorus is one-tenth of the overall content of the nutrient with a maximum of ·87% by weight, provided that the overall content of the nutrient remains within the limits specified in Annex I and the tolerances specified in paragraph (e) above.

PART IV.

CERTIFICATE OF RESULT OF ANALYSIS OF A FERTILISER.

Sample of.............................marked................

received by the Analyst on .......................................from .........................................

which was taken at the premises of............................................................ ................

This is to certify that the above-mentioned sample which was duly fastened and sealed, has been analysed by........................ under the direction of the State Chemist, and that the result of the analysis is as follows:

Per Cent

Total Nitrogen (N)

.........................................

Ammoniacal Nitrogen (N)

.........................................

Nitric Nitrogen (N)

..........................................

Ureic Nitrogen (N)

..........................................

Cyanamide Nitrogen (N)

..........................................

Phosphorus (P) soluble in neutral Ammonium Citrate and in water

...........................................

Phosphorus (P) soluble in water

...........................................

Phosphorus (P) soluble in neutral Ammonium Citrate

..........................................

Phosphorus (P) soluble in mineral acids only

.........................................

Phosphorus (P) soluble in Alkaline Ammonium Citrate (Petermann)

.........................................

Phosphorus (P) soluble in 2 % citric acid

............................................

Phosphorus (P) soluble in mineral acids, of which at least 75 % of the declared phosphorus content is soluble in Alkaline Ammonium Citrate (Joulie)

..............................................

Phosphorus (P) soluble in mineral acids, of which at least 55 % of the declared phosphorus content is soluble in 2 % formic acid

........................................

Potassium (K) soluble in water

.........................................

Water soluble Magnesium (Mg) salts expressed as Magnesium

.............................................

Total Magnesium (Mg)

..........................................

Chlorine (C)

...............................................

Amount found to pass through a 0·160 mm sieve

.............................................

Amount found to pass through a 0·063 mm sieve

..............................................

On comparison of the results of the analysis with the particulars accompanying the sample it appears that the particulars furnished:—

*are correct, subject to the prescribed tolerance limits

*are not correct subject to the prescribed tolerance limits, in the following respects:—

This Certificate is given under Section   of the

Date .................................................

Signed ..........................................................

State Chemist

*Delate as appropriate

GIVEN under my Official Seal, this 19th day of January, 1978.

JAMES GIBBONS,

Minister for Agriculture.

EXPLANATORY NOTE

The Regulations—

(1) provide for a designation "EEC fertiliser",

(2) lay down criteria with which fertilisers marketed under the designation 'EEC fertiliser' must comply.